In this research work,spent silicon contact mass and chlorine gas were used to synthesize tetrachlorosilane via the fluidized bed technique. On the base of fluidization of fine powders, the synthesis condition experiments, fluidized bed structures, heat change modes are researched simultaneously by the two fluidized beds. Via the discussion of reaction mechanism, research direction was determined. After the technology was magnified,the experimental results were tested and proved to be corrected. The major influential factors of the reaction were analyzed. Tetrachlorosilane is the main material during the production of fumed silica, on the other hand the application of fumed silica production is extensive and optimistic.
YAN Shi-cheng.
Study on New Technology of Synthesis Silicon? Tetrachloride from Abandoned Catalyst in Direct Synthesis of Tetrachlorosilane. Journal of Northeast Electric Power University. 2010, 30(6): 36-39